wv_cooker wrote:You have several things to think of here and first let me say I have no understanding of the type Still you are experimenting with.
3. As we all know the wash temp takes care of itself in the boiler and by the same token the fractions take care of them selves in the column. This only leaves one thing that can be controlled accurately in my opinion and that is coolant. How to do this, control the deph coolant by coolant temp to accurately set the reflux rate. And secondly control the Product condenser coolant to keep the product as cool as possible. In my opinion this would make a better product with less smearing than any other method. Just my thoughts hope it helps.
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